Please use this identifier to cite or link to this item: https://idr.l2.nitk.ac.in/jspui/handle/123456789/14848
Title: High-yielding synthesis of alkyl stearates from stearic acid within a closed batch reactor using heteropolyacids as efficient and recyclable catalyst
Authors: Vinod N.
Tiwari R.
Bhat N.S.
Mal S.S.
Dutta, Saikat
Issue Date: 2020
Citation: AIP Conference Proceedings , Vol. 2225 , , p. -
Abstract: This study reports high-yielding and scalable synthesis of alkyl stearates from stearic acid (SA) within a closed batch reactor using commercially-available heteropolyacid catalysts. The reaction was carried out by using different commercially-available heteropolyacids and reaction conditions were optimized by using phosphotungstic acid (PTA) catalyst. The solvent-free, gram-scale reactions afforded alkyl stearates in excellent isolated yields (>95%) within 4?h at 110 °C using slight excess of alcohols and only 1?mol% of the phosphotungstic acid (PTA) catalyst. The PTA catalyst was successfully recovered and reused for five consecutive cycles without significant loss in mass or activity. © 2020 Author(s).
URI: https://doi.org/10.1063/5.0005580
https://idr.nitk.ac.in/jspui/handle/123456789/14848
Appears in Collections:2. Conference Papers

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